Information card for entry 2020525

Structure parameters

• Chemical name: <i>catena</i>-Poly[[copper(II)-di-μ-chlorido-copper(II)-{μ-1-ethyl-<i>N</i>'-[(1<i>H</i>-imidazol-3-yl)methylidene]-7-methyl-4-oxo-1,4-dihydro-1,8-naphthyridine-3-carbohydrazidato}-[dimethanolcopper(II)]-{μ-1-ethyl-<i>N</i>'-[(1<i>H</i>-imidazol-3-yl)methylidene]-7-methyl-4-oxo-1,4-dihydro-1,8-naphthyridine-3-carbohydrazidato}] dichloride methanol tetrasolvate]
• Formula: C18 H23 Cl2 Cu1.5 N6 O4
• Calculated formula: C36 H46 Cl4 Cu3 N12 O8
• Title of publication: A novel binuclear copper complex incorporating a nalidixic acid derivative displaying a one-dimensional coordination polymeric structure
• Authors of publication: Bergamini, F. R. G.; Ribeiro, M. A.; Miranda, P. C. M. L.; Formiga, A. L. B.; Corbi, P. P.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 7
• Pages of publication: 544 - 548
• a: 18.5958 ± 0.0011 Å
• b: 16.6608 ± 0.001 Å
• c: 14.2394 ± 0.0009 Å
• α: 90°
• β: 93.692 ± 0.002°
• γ: 90°
• Cell volume: 4402.5 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0343
• Residual factor for significantly intense reflections: 0.0274
• Weighted residual factors for significantly intense reflections: 0.0703
• Weighted residual factors for all reflections included in the refinement: 0.0739
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes