Information card for entry 2020527

Structure parameters

• Chemical name: Bis[μ~2~-<i>N</i>'-(2-oxidobenzylidene)benzohydrazidato-κ^4^<i>O</i>:<i>O</i>,<i>N</i>',<i>O</i>']dilead(II)
• Formula: C28 H20 N4 O4 Pb2
• Calculated formula: C28 H20 N4 O4 Pb2
• SMILES: c12ccccc1C=[N]1N=C(O[Pb]31[O]2[Pb]12[N](=Cc4c(cccc4)[O]31)N=C(c1ccccc1)O2)c1ccccc1
• Title of publication: Intermolecular Pb···N interactions in lead(II) dimers producing a supramolecular two-dimensional metal‒organic compound: bis[μ~2~-<i>N</i>'-(2-oxidobenzylidene)benzohydrazidato-κ^4^<i>O</i>:<i>O</i>,<i>N</i>',<i>O</i>']dilead(II)
• Authors of publication: Schwade, Vânia Denise; Faoro, Eliandro; Schulz Lang, Ernesto
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2016
• Journal volume: 72
• Journal issue: 7
• Pages of publication: 525 - 529
• a: 8.3754 ± 0.0007 Å
• b: 12.6354 ± 0.001 Å
• c: 13.6686 ± 0.0011 Å
• α: 112.213 ± 0.003°
• β: 101.395 ± 0.003°
• γ: 95.781 ± 0.003°
• Cell volume: 1287.99 ± 0.19 ų
• Cell temperature: 300 ± 2 K
• Ambient diffraction temperature: 300 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0251
• Residual factor for significantly intense reflections: 0.0177
• Weighted residual factors for significantly intense reflections: 0.0354
• Weighted residual factors for all reflections included in the refinement: 0.037
• Goodness-of-fit parameter for all reflections included in the refinement: 1.068
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes