Crystallography Open Database

Information card for entry 2021260

2021259 << 2021260 >> 2021261

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Structure parameters

Chemical name	Heptaammonium nitratotetradecavanadate dimethyl sulfoxide hexasolvate
Formula	C12 H64 N8 O47 S6 V14
Calculated formula	C12 H64 N8 O47 S6 V14
Title of publication	Synthesis and structural characterization of tube-type tetradecavanadates
Authors of publication	Kuwajima, Sho; Arai, Yuta; Kitajima, Hiromasa; Kikukawa, Yuji; Hayashi, Yoshihito
Journal of publication	Acta Crystallographica Section C
Year of publication	2018
Journal volume	74
Journal issue	11
a	19.3923 ± 0.0007 Å
b	24.9031 ± 0.0009 Å
c	14.5785 ± 0.0005 Å
α	90°
β	116.374 ± 0.001°
γ	90°
Cell volume	6307.6 ± 0.4 Å³
Cell temperature	90 ± 2 K
Ambient diffraction temperature	90 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0577
Residual factor for significantly intense reflections	0.0522
Weighted residual factors for significantly intense reflections	0.1327
Weighted residual factors for all reflections included in the refinement	0.1376
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	Yes

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