Information card for entry 2022538

Structure parameters

• Common name: (18-Crown-6)bis(tetrahydrofuran)potassium bis(η^4^-anthracene)(trimethylphosphane)vanadium tetrahydrofuran monosolvate
• Chemical name: (1,4,7,10,13,16-Hexaoxacyclooctadecane)bis(tetrahydrofuran)potassium bis(η^4^-anthracene)(trimethylphosphane)vanadium tetrahydrofuran monosolvate
• Formula: C55 H77 K O9 P V
• Calculated formula: C55.004 H77.008 K O9.001 P V
• Title of publication: Syntheses and crystal structures of new naphthalene– and anthracene–vanadate salts and an unprecedented dimetallabis(anthracene) sandwich complex: [Na(tetrahydrofuran)~3~][V~2~(anthracene)~2~]
• Authors of publication: Kucera, Benjamin E.; Young, Jr, Victor G.; Brennessel, William W.; Ellis, John E.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2022
• Journal volume: 78
• Journal issue: 3
• a: 9.6431 ± 0.0012 Å
• b: 14.4883 ± 0.0018 Å
• c: 20.804 ± 0.003 Å
• α: 74.992 ± 0.002°
• β: 84.667 ± 0.002°
• γ: 71.815 ± 0.002°
• Cell volume: 2667 ± 0.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0849
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for significantly intense reflections: 0.1068
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes