Information card for entry 2022645

Structure parameters

• Chemical name: <i>catena</i>-Poly[[(5,5'-dimethyl-2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')iron(II)]-di-μ-azido-κ^2^<i>N</i>^1^:<i>N</i>^3^-[(5,5'-dimethyl-2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')iron(II)]-di-μ-azido-κ^2^<i>N</i>^1^:<i>N</i>^1^]
• Formula: C12 H12 Fe N8
• Calculated formula: C12 H12 Fe N8
• Title of publication: Concomitant dimorphism in poly[di-μ-azido-(5,5'-dimethyl-2,2'-bipyridine)iron(II)]
• Authors of publication: Setifi, Zouaoui; Bernès, Sylvain; Geiger, David K.; Setifi, Fatima; Reedijk, Jan
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2022
• Journal volume: 78
• Journal issue: 8
• a: 7.7235 ± 0.0007 Å
• b: 9.4051 ± 0.0007 Å
• c: 10.5846 ± 0.0009 Å
• α: 112.585 ± 0.003°
• β: 102.828 ± 0.004°
• γ: 92.852 ± 0.003°
• Cell volume: 684.36 ± 0.1 ų
• Cell temperature: 298 ± 1 K
• Ambient diffraction temperature: 298 ± 1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0782
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.1037
• Weighted residual factors for all reflections included in the refinement: 0.1281
• Goodness-of-fit parameter for all reflections included in the refinement: 1.141
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes