Information card for entry 2023143

Structure parameters

• Chemical name: Pentasodium nonadecacesium tetracosatungstate(VI) heneikosahydrate
• Formula: Cs19 H42 Na5 O105 W24
• Calculated formula: Cs19 Na4.9999 O105 W24
• Title of publication: Synthesis and structural characterization of a hydrated sodium–caesium tetracosatungstate(VI), Na5Cs19[W24O84]·21H2O
• Authors of publication: Deblonde, Gauthier; Colliard, Ian
• Journal of publication: Acta Crystallographica Section E Crystallographic Communications
• Year of publication: 2024
• Journal volume: 80
• Journal issue: 6
• Pages of publication: 667 - 670
• a: 18.0071 ± 0.0003 Å
• b: 18.0071 ± 0.0003 Å
• c: 62.9142 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 17667.2 ± 0.5 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0645
• Residual factor for significantly intense reflections: 0.0617
• Weighted residual factors for significantly intense reflections: 0.1669
• Weighted residual factors for all reflections included in the refinement: 0.1704
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No