Information card for entry 2023275

Structure parameters

• Chemical name: (μ-Tetrathioantimonato-κ^2^<i>S</i>:<i>S</i>')bis[(1,4,8,11-tetraazacyclotetradecane-κ^4^<i>N</i>)zinc(II)] perchlorate 0.8-hydrate
• Formula: C20 H49.6 Cl N8 O4.8 S4 Sb Zn2
• Calculated formula: C20 H49.6 Cl N8 O4.8 S4 Sb Zn2
• Title of publication: Synthesis, crystal structure and properties of μ-tetrathioantimonato-bis[(cyclam)zinc(II)] perchlorate 0.8-hydrate
• Authors of publication: Näther, Christian; Lühmann, Henning; Bensch, Wolfgang
• Journal of publication: Acta Crystallographica Section E Crystallographic Communications
• Year of publication: 2024
• Journal volume: 80
• Journal issue: 11
• Pages of publication: 1151 - 1156
• a: 9.11238 ± 0.00007 Å
• b: 13.67434 ± 0.0001 Å
• c: 27.49214 ± 0.00018 Å
• α: 90°
• β: 92.9206 ± 0.0006°
• γ: 90°
• Cell volume: 3421.23 ± 0.04 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 7
• Hermann-Mauguin space group symbol: P 1 c 1
• Hall space group symbol: P -2yc
• Residual factor for all reflections: 0.0238
• Residual factor for significantly intense reflections: 0.0227
• Weighted residual factors for significantly intense reflections: 0.0577
• Weighted residual factors for all reflections included in the refinement: 0.0582
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No