Hydrogen-bonding behaviour of benzene-1,2,4,5-tetracarboxylic acid: supramolecular structures of different dimensionality in the 2:1 adducts formed with 4,4'-bipyridyl and hexamethylenetetramine
Authors of publication
Lough, Alan J.; Wheatley, Paul S.; Ferguson, George; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section B
Year of publication
2000
Journal volume
56
Journal issue
2
Pages of publication
261 - 272
a
9.7029 ± 0.0006 Å
b
10.9369 ± 0.0007 Å
c
16.7647 ± 0.0011 Å
α
84.271 ± 0.003°
β
79.399 ± 0.003°
γ
75.264 ± 0.003°
Cell volume
1688.55 ± 0.19 Å3
Cell temperature
100 ± 1 K
Ambient diffraction temperature
100 ± 1 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1262
Residual factor for significantly intense reflections
0.0482
Weighted residual factors for all reflections included in the refinement
0.1142
Goodness-of-fit parameter for all reflections included in the refinement
