Information card for entry 2102685

Structure parameters

• Common name: Palladium diethylphenylazothioformaide
• Chemical name: Trans-(di(N,N-diethyl-(2-phenyldiazenyl)thioformamide-κS,κN^2^))palladium
• Formula: C22 H30 N6 Pd S2
• Calculated formula: C22 H30 N6 Pd S2
• SMILES: c1ccccc1[N]1[Pd]2([S]=C(N=1)N(CC)CC)[S]=C(N=[N]2c1ccccc1)N(CC)CC
• Title of publication: Structural study of four complexes of the <i>M</i>-N~2~S~2~ type derived from diethylphenylazothioformamide and the metals palladium, platinum, copper and nickel
• Authors of publication: Nielsen, Kim T.; Harris, Pernille; Bechgaard, Klaus; Krebs, Frederik C.
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 1
• Pages of publication: 151 - 156
• a: 16.036 ± 0.0016 Å
• b: 12.4564 ± 0.0013 Å
• c: 12.3311 ± 0.0012 Å
• α: 90°
• β: 100.952 ± 0.002°
• γ: 90°
• Cell volume: 2418.3 ± 0.4 ų
• Cell temperature: 118 K
• Ambient diffraction temperature: 118 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0604
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for significantly intense reflections: 0.1008
• Weighted residual factors for all reflections included in the refinement: 0.1051
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No