Information card for entry 2103748

Structure parameters

• Common name: [CA10]
• Chemical name: [Cyclodecaamylose].27.18 H2 O
• Formula: C60 H153.42 O77.18
• Calculated formula: C60 H153.42 O77.18
• Title of publication: Hydrogen-bond network in cyclodecaamylose hydrate at 20K; neutron diffraction study of novel structural motifs band-flip and kink in α-(1→4)-<small>D</small>-glucoside oligosaccharides
• Authors of publication: Imamura, K.; Nimz, O.; Jacob, J.; Myles, D.; Mason, S. A.; Kitamura, S.; Aree, T.; Saenger, W.
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2001
• Journal volume: 57
• Journal issue: 6
• Pages of publication: 833 - 841
• a: 29.31 ± 0.05 Å
• b: 9.976 ± 0.01 Å
• c: 19.34 ± 0.02 Å
• α: 90°
• β: 121.07 ± 0.02°
• γ: 90°
• Cell volume: 4844 ± 11 ų
• Cell temperature: 20 ± 2 K
• Ambient diffraction temperature: 20 ± 2 K
• Number of distinct elements: 3
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0681
• Residual factor for significantly intense reflections: 0.0635
• Weighted residual factors for all reflections included in the refinement: 0.1477
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation probe: neutron
• Diffraction radiation wavelength: 1.532 Å
• Diffraction radiation type: neutron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No