Syntheses, spectroscopic study and X-ray crystallography of some new phosphoramidates and lanthanide(III) complexes of <i>N</i>-(4-nitrobenzoyl)-<i>N</i>',<i>N</i>''-bis(morpholino)phosphoric triamide
Authors of publication
Gholivand, Khodayar; Mostaanzadeh, Hossein; Koval, Tomas; Dusek, Michal; Erben, Mauricio F.; Stoeckli-Evans, Helen; Della Védova, Carlos O.
Journal of publication
Acta Crystallographica Section B
Year of publication
2010
Journal volume
66
Journal issue
4
Pages of publication
441 - 450
a
8.8631 ± 0.001 Å
b
33.466 ± 0.004 Å
c
15.5399 ± 0.0018 Å
α
90°
β
93.195 ± 0.003°
γ
90°
Cell volume
4602.2 ± 0.9 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0799
Residual factor for significantly intense reflections
0.0554
Weighted residual factors for significantly intense reflections
0.1022
Weighted residual factors for all reflections included in the refinement
0.1118
Goodness-of-fit parameter for all reflections included in the refinement
