Information card for entry 2105973

Structure parameters

• Formula: C28 H40 F12 N18 O6 Rh2 Si2
• Calculated formula: C28 H28 F12 N18 O6 Rh2 Si2
• SMILES: [Rh]12([n]3c([nH]cc3)c3[n]1cc[nH]3)([n]1c([nH]cc1)c1[n]2cc[nH]1)([Rh]12([n]3c([nH]cc3)c3[n]1cc[nH]3)([n]1c([nH]cc1)c1[n]2cc[nH]1)[n]1cc[n](cc1)[Rh]12([n]3c([nH]cc3)c3[n]1cc[nH]3)([n]1c([nH]cc1)c1[n]2cc[nH]1)[Rh]12([n]3c([nH]cc3)c3[n]1cc[nH]3)[n]1c([nH]cc1)c1[n]2cc[nH]1)[n]1ccncc1.[Si](F)(F)(F)(F)([F-])[F-].[Si](F)(F)(F)(F)([F-])[F-].O.O.O.O.O.O.[Si](F)(F)(F)(F)([F-])[F-].[Si](F)(F)(F)(F)([F-])[F-].O.O.O.O.O.O
• Title of publication: Assembled structures of tetrakis(biimidazole)dirhodium complexes hydrogen-bonded with common inorganic anions
• Authors of publication: Jin-Long; Uemura, Kazuhiro; Ebihara, Masahiro
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2014
• Journal volume: 70
• Journal issue: 6
• Pages of publication: 1006 - 1019
• a: 27.057 ± 0.005 Å
• b: 9.9832 ± 0.0015 Å
• c: 18.718 ± 0.003 Å
• α: 90°
• β: 122.256 ± 0.0019°
• γ: 90°
• Cell volume: 4275.7 ± 1.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0522
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for significantly intense reflections: 0.1327
• Weighted residual factors for all reflections included in the refinement: 0.1364
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No