Information card for entry 2108746

Structure parameters

• Chemical name: Ammonium tris(2,2'-bipyridine)cobaltate(II) octamolybdate tetrahydrate
• Formula: C30 H36 Co Mo8 N7 O30
• Calculated formula: C30 H36 Co Mo8 N7 O30
• Title of publication: Concomitance of octamolybdate isomers in metastable crystal structures isolated using homoleptic Co^II^/Co^III^ complexes as structure-directing templates
• Authors of publication: Atencio, Reinaldo; Briceño, Alexander; Bruno-Colmenarez, Julia; Silva, Pedro; Rodríguez, Laura; Sosa, Eleida; Limones, Erick; Pacheco, Yesenia; Cáceres, Julio; Vielma, Joel
• Journal of publication: Acta Crystallographica Section B
• Year of publication: 2021
• Journal volume: 77
• Journal issue: 1
• Pages of publication: 99 - 114
• a: 19.27 ± 0.003 Å
• b: 10.993 ± 0.002 Å
• c: 23.917 ± 0.003 Å
• α: 90°
• β: 107.517 ± 0.011°
• γ: 90°
• Cell volume: 4831.5 ± 1.3 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0427
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.065
• Weighted residual factors for all reflections included in the refinement: 0.0703
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes