Information card for entry 2200708

Structure parameters

• Chemical name: trans-Dichloro(meso-2,3,7,11,12-pentamethyl-3,7,11,17-tetra- azabicyclo[11.3.1]heptadeca-1(17),13,15-triene-κ^4^N^3,7,11,17^)rhodium(III) hexafluorphosphate
• Formula: C18 H32 Cl2 F6 N4 P Rh
• Calculated formula: C18 H32 Cl2 F6 N4 P Rh
• Title of publication: <i>trans</i>-Dichloro(<i>meso</i>-2,3,7,11,12-pentamethyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene-κ^4^<i>N</i>^3,7,11,17^)rhodium(III) hexafluorophosphate
• Authors of publication: Blake, Alexander J.; Hyde, Timothy I.; Schröder, Martin
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2001
• Journal volume: 57
• Journal issue: 10
• Pages of publication: m459 - m461
• a: 7.949 ± 0.005 Å
• b: 11.067 ± 0.005 Å
• c: 14.116 ± 0.005 Å
• α: 74.22 ± 0.05°
• β: 86.26 ± 0.05°
• γ: 84.67 ± 0.05°
• Cell volume: 1188.8 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0934
• Residual factor for significantly intense reflections: 0.0649
• Weighted residual factors for all reflections included in the refinement: 0.182
• Goodness-of-fit parameter for all reflections included in the refinement: 0.996
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes