Information card for entry 2202741

Structure parameters

• Chemical name: diaquabis[dimethylglyoximato(2-)]bis[dimethylglyoximato(1-)] bis(phenanthroline)tetracopper(II) bis[dimethylglyoximato(2-)]bis[dimethylglyoximato(1-)] bis(phenanthroline)tetracopper(II) tetraperchlorate methanol disolvate
• Formula: C82 H96 Cl4 Cu8 N24 O36
• Calculated formula: C82 H88 Cl4 Cu8 N24 O36
• Title of publication: A new tetranuclear copper(II) complex bridged by dimethylglyoxime
• Authors of publication: Zhang, Baofeng; Chu, Sheng; Wang, Xiaoqing; Shen, Guangqiu; Wang, Ru-Ji
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 7
• Pages of publication: m504 - m506
• a: 13.922 ± 0.003 Å
• b: 14.841 ± 0.004 Å
• c: 15.024 ± 0.004 Å
• α: 65.547 ± 0.005°
• β: 70.265 ± 0.005°
• γ: 67.182 ± 0.004°
• Cell volume: 2545.9 ± 1.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1123
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1328
• Weighted residual factors for all reflections included in the refinement: 0.1593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes