Information card for entry 2203288

Structure parameters

• Chemical name: [1,8-Di-2-n-propyl-1,3,6,8,10,13-hexaazacyclotetradecane]nickel(II) diperchlorate
• Formula: C14 H34 Cl2 N6 Ni O8
• Calculated formula: C14 H34 Cl2 N6 Ni O8
• Title of publication: (1,8-Di-<i>n</i>-propyl-1,3,6,8,10,13-hexaazacyclotetradecane)nickel(II) diperchlorate
• Authors of publication: Li, Yan-Wu; Xiang, Hua; Lu, Tong-Bu; Ng, Seik Weng
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 3
• Pages of publication: m312 - m313
• a: 8.1634 ± 0.0006 Å
• b: 12.411 ± 0.001 Å
• c: 12.518 ± 0.001 Å
• α: 77.094 ± 0.001°
• β: 83.348 ± 0.001°
• γ: 71.882 ± 0.001°
• Cell volume: 1173.47 ± 0.16 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0532
• Residual factor for significantly intense reflections: 0.0438
• Weighted residual factors for significantly intense reflections: 0.1238
• Weighted residual factors for all reflections included in the refinement: 0.1305
• Goodness-of-fit parameter for all reflections included in the refinement: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes