Information card for entry 2203888

Structure parameters

• Chemical name: Bis[μ^2^-bis(diphenylphosphinoyl)methanido-κ^2^O:O']hexamethyldi-μ^3^-oxo- dialuminium(III) tetrahydrofuran disolvate
• Formula: C64 H76 Al4 O8 P4
• Calculated formula: C56 H60 Al4 O6 P4
• SMILES: c1ccccc1P1(=[O][Al]([O]2[Al]3(OP(=C1)(c1ccccc1)c1ccccc1)([O]1[Al]([O]=P(c4ccccc4)(c4ccccc4)C=P(O[Al]231C)(c1ccccc1)c1ccccc1)(C)C)C)(C)C)c1ccccc1
• Title of publication: Bis[μ^2^-bis(diphenylphosphinoyl)methanido-κ^2^<i>O</i>:<i>O</i>']hexamethyldi-μ^3^-oxo-tetraaluminium(III) tetrahydrofuran disolvate
• Authors of publication: Nassar, Roger; Noll, Bruce C.; Henderson, Kenneth W.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 7
• Pages of publication: m1023 - m1024
• a: 13.0087 ± 0.0002 Å
• b: 18.5644 ± 0.0003 Å
• c: 13.7312 ± 0.0002 Å
• α: 90°
• β: 102.117 ± 0.001°
• γ: 90°
• Cell volume: 3242.19 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0757
• Residual factor for significantly intense reflections: 0.0615
• Weighted residual factors for significantly intense reflections: 0.1657
• Weighted residual factors for all reflections included in the refinement: 0.1734
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes