Information card for entry 2203962

Structure parameters

• Common name: [(tmedaH2){V2Cl5(tmeda)2}][BPh4].(THF)
• Formula: C46 H78 B Cl5 N6 O V2
• Calculated formula: C46 H78 B Cl5 N6 O V2
• Title of publication: <i>N,N,N</i>',<i>N</i>'-Tetramethylethane-1,2-diaminium tri-μ-chloro-bis[(<i>N,N,N</i>',<i>N</i>'-tetramethylethane-1,2-diamine)vanadium(II)] tetraphenylborate tetrahydrofuran solvate
• Authors of publication: Raimondi, Angela Cristina; Hasegawa, Tai; Nunes, Fábio Souza
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 7
• Pages of publication: m1010 - m1012
• a: 9.3902 ± 0.0017 Å
• b: 14.9426 ± 0.0013 Å
• c: 19.455 ± 0.004 Å
• α: 102.125 ± 0.014°
• β: 98.065 ± 0.017°
• γ: 92.267 ± 0.011°
• Cell volume: 2635.8 ± 0.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1019
• Weighted residual factors for all reflections included in the refinement: 0.1182
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes