Information card for entry 2204320

Structure parameters

• Chemical name: (Acetato-κO)[butane-2,3-dione monooxime benzoylhydrazonato-κ^3^O,N^2^,O']bis(pyridine-κN)nickel(II)
• Formula: C23 H25 N5 Ni O4
• Calculated formula: C23 H25 N5 Ni O4
• SMILES: [Ni]12([N](O)=C(C(=[N]1N=C(O2)c1ccccc1)C)C)([n]1ccccc1)([n]1ccccc1)OC(=O)C
• Title of publication: (Acetato-κ<i>O</i>)[butane-2,3-dione monooxime benzoylhydrazonato-κ^3^<i>O</i>,<i>N</i>^2^,<i>O</i>']bis(pyridine-κ<i>N</i>)nickel(II)
• Authors of publication: Huo, Li-Hua; Lu, Zhen-Zhong; Gao, Shan; Zhao, Hui
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 10
• Pages of publication: m1450 - m1452
• a: 12.378 ± 0.001 Å
• b: 14.77 ± 0.001 Å
• c: 13.3291 ± 0.0007 Å
• α: 90°
• β: 99.073 ± 0.004°
• γ: 90°
• Cell volume: 2406.4 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.049
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.083
• Weighted residual factors for all reflections included in the refinement: 0.087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes