Information card for entry 2204718

Structure parameters

• Chemical name: (2R)-2-N-(tert-Butoxycarbonyl)-Amino-3-Methyl-1,3-Butanediol
• Formula: C10 H21 N O4
• Calculated formula: C10 H21 N O4
• Title of publication: A synthetic intermediate of enantiopure <i>N</i>-protected β-hydroxyvaline, (2<i>R</i>)-2-[<i>N</i>-(<i>tert</i>-butoxycarbonyl)amino]-3-methylbutane-1,3-diol
• Authors of publication: Oku, Hiroyuki; Naito, Ryo; Yamada, Keiichi; Katakai, Ryoichi
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2004
• Journal volume: 60
• Journal issue: 12
• Pages of publication: o2462 - o2464
• a: 9.833 ± 0.008 Å
• b: 18.994 ± 0.017 Å
• c: 6.713 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1254 ± 2 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 4
• Space group number: 18
• Hermann-Mauguin space group symbol: P 21 21 2
• Hall space group symbol: P 2 2ab
• Residual factor for significantly intense reflections: 0.085
• Weighted residual factors for all reflections included in the refinement: 0.244
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No