Information card for entry 2208321

Structure parameters

• Chemical name: (diethyl ether)(μ~4~-2-{6-[1,3-dimethyl-3-(2-pyridyl)-1,4-bis(2,4,6- trimethylanilinio)butyl]-2-pyridyl}-2-methyl-1,3-bis(2,4,6- trimethylanilinio)propane)tetralithium(I) diethyl ether solvate
• Formula: C59 H74 Li4 N6 O
• Calculated formula: C59 H74 Li4 N6 O
• Title of publication: Lithiation of the diaminopyridine protio-ligand MeC(2-C~5~H~4~N){CH~2~N(H)Mes}~2~ (Mes = 2,4,6-C~6~H~2~Me~3~)
• Authors of publication: Ward, Benjamin D.; Gade, Lutz H.; Mountford, Philip
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 3
• Pages of publication: m472 - m474
• a: 11.607 ± 0.002 Å
• b: 14.302 ± 0.003 Å
• c: 17.477 ± 0.004 Å
• α: 78.18 ± 0.03°
• β: 72.68 ± 0.03°
• γ: 80.31 ± 0.03°
• Cell volume: 2693 ± 1.1 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1479
• Residual factor for significantly intense reflections: 0.0511
• Weighted residual factors for all reflections: 0.1378
• Weighted residual factors for significantly intense reflections: 0.0537
• Weighted residual factors for all reflections included in the refinement: 0.0537
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0869
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes