Information card for entry 2208400

Structure parameters

• Common name: Dichloro-O-(dimethylformamide)[hydrotris(pyrazol-1-yl)borato]vanadium(III) Chloro-O-(N,N-dimethylformamide)[hydrotris(pyrazol-1-yl)borato]oxovanadium(IV)
• Chemical name: dichloro(N,N-dimethylformamide)[hydrotris(pyrazol-1-yl)borato]vanadium(III) chloro(N,N-dimethylformamide)[hydrotris(pyrazol-1-yl)borato]oxovanadium(IV)
• Formula: C24 H34 B2 Cl3.06 N14 O2.94 V2
• Calculated formula: C24 H34 B2 Cl3.06 N14 O2.94 V2
• Title of publication: Cocrystallization of dichloro(<i>N</i>,<i>N</i>-dimethylformamide)[hydrotris(pyrazol-1-yl)borato]vanadium(III) with its partially oxidized analog chloro(<i>N</i>,<i>N</i>-dimethylformamide)[hydrotris(pyrazol-1-yl)borato]oxovanadium(IV)
• Authors of publication: McLauchlan, Craig C.; McDonald, Kenneth J.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 3
• Pages of publication: m588 - m590
• a: 8.6005 ± 0.0005 Å
• b: 13.7002 ± 0.001 Å
• c: 14.8204 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1746.3 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0583
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.1278
• Weighted residual factors for all reflections included in the refinement: 0.1337
• Goodness-of-fit parameter for all reflections included in the refinement: 1.103
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes