Information card for entry 2208887

Structure parameters

• Chemical name: Di-μ~2~-chloro-1:2κ^2^Cl,3:4κ^2^Cl-chloro-4κCl-(6-chloropyridine- 3-carboxylato-1κ^2^O,O')octamethyl-1κ^2^C,2κ^2^C,3κ^2^C,4κ^2^C- di-μ~3~-oxo-1:2:3κ^3^O,2:3:4κ^3^O-tetratin(IV) diethyl ether solvate
• Formula: C18 H37 Cl4 N O5 Sn4
• Calculated formula: C14 H27 Cl4 N O4 Sn4
• SMILES: [Sn]12([Cl][Sn]3(C)(C)[O]1[Sn]1([Cl][Sn](Cl)(C)(C)[O]31)(C)C)(C)(C)OC(=[O]2)c1cnc(Cl)cc1
• Title of publication: Di-μ~2~-chloro-1:2κ^2^<i>Cl</i>,3:4κ^2^<i>Cl</i>-chloro-4κ<i>Cl</i>-(6-chloropyridine-3-carboxylato-1κ^2^<i>O</i>,<i>O</i>')octamethyl-1κ^2^<i>C</i>,2κ^2^<i>C</i>,3κ^2^<i>C</i>,4κ^2^<i>C</i>-di-μ~3~-oxo-1:2:3κ^3^<i>O</i>,2:3:4κ^3^<i>O</i>-tetratin(IV) diethyl ether solvate
• Authors of publication: Fa-Hui li; Han-Dong Yin; Qiang Zhao; Wen-Li Liu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 5
• Pages of publication: m1117 - m1118
• a: 16.123 ± 0.002 Å
• b: 11.0953 ± 0.0015 Å
• c: 20.309 ± 0.003 Å
• α: 90°
• β: 113.059 ± 0.002°
• γ: 90°
• Cell volume: 3342.8 ± 0.8 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0604
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0777
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes