Information card for entry 2209249

Structure parameters

• Common name: [(dppe)P 1+]2 [SnCl6 2-] . 2 CH2Cl2
• Chemical name: bis[1,1,3,3-tetraphenyl-1,3,2-triphospholenylium] hexachlorostannate dichloromethane solvate
• Formula: C54 H52 Cl10 P6 Sn
• Calculated formula: C54 H52 Cl10 P6 Sn
• SMILES: C1CP(=P[P+]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.C(Cl)Cl.Cl[Sn](Cl)([Cl-])(Cl)(Cl)[Cl-].C1CP(=P[P+]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.C(Cl)Cl
• Title of publication: Redetermination of a cyclic triphosphenium hexachlorostannate salt at 173 K
• Authors of publication: Ellis, Bobby D.; Macdonald, Charles L. B.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 6
• Pages of publication: m1235 - m1236
• a: 10.8589 ± 0.0004 Å
• b: 11.5303 ± 0.0005 Å
• c: 13.0841 ± 0.0005 Å
• α: 68.777 ± 0.001°
• β: 79.774 ± 0.001°
• γ: 81.332 ± 0.001°
• Cell volume: 1496.16 ± 0.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.0539
• Weighted residual factors for significantly intense reflections: 0.1015
• Weighted residual factors for all reflections included in the refinement: 0.1121
• Goodness-of-fit parameter for all reflections included in the refinement: 1.234
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes