Information card for entry 2209694

Structure parameters

• Chemical name: [N,N,N'-Tris(3-aminopropyl)ethylenediamine-κ^5^N]nickel bis(perchlorate)
• Formula: C11 H29 Cl2 N5 Ni O8
• Calculated formula: C11 H29 Cl2 N5 Ni O8
• Title of publication: [<i>N</i>,<i>N</i>,<i>N</i>'-Tris(3-aminopropyl)ethylenediamine-κ^5^<i>N</i>]nickel bis(perchlorate)
• Authors of publication: Xu, Tong-Tao; Xu, Xing-You; Wang, Da-Qi; Gao, Jian; Lu, Lu-De
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 7
• Pages of publication: m1713 - m1715
• a: 9.454 ± 0.004 Å
• b: 14.589 ± 0.007 Å
• c: 14.477 ± 0.007 Å
• α: 90°
• β: 90.285 ± 0.008°
• γ: 90°
• Cell volume: 1996.7 ± 1.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1944
• Residual factor for significantly intense reflections: 0.0637
• Weighted residual factors for significantly intense reflections: 0.1066
• Weighted residual factors for all reflections included in the refinement: 0.1311
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes