Information card for entry 2210312

Structure parameters

• Chemical name: Tetrakis(2,3,5,6-tetrafluorobenzenethiolato-κS)(triphenylphosphine- κP)osmium(IV) n-hexane hemisolvate
• Formula: C45 H26 F16 Os P S4
• Calculated formula: C45 H26 F16 Os P S4
• Title of publication: Tetrakis(2,3,5,6-tetrafluorobenzenethiolato-κ<i>S</i>)(triphenylphosphine-κ<i>P</i>)osmium(IV) <i>n</i>-hexane hemisolvate
• Authors of publication: Cerón, Margarita; Arroyo, Maribel; Bernès, Sylvain
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 9
• Pages of publication: m2167 - m2169
• a: 12.209 ± 0.003 Å
• b: 13.513 ± 0.003 Å
• c: 13.865 ± 0.003 Å
• α: 89.2 ± 0.02°
• β: 87.4 ± 0.02°
• γ: 86.454 ± 0.015°
• Cell volume: 2280.6 ± 0.9 ų
• Cell temperature: 296 ± 1 K
• Ambient diffraction temperature: 296 ± 1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0841
• Residual factor for significantly intense reflections: 0.0645
• Weighted residual factors for significantly intense reflections: 0.1608
• Weighted residual factors for all reflections included in the refinement: 0.174
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes