Information card for entry 2211224

Structure parameters

• Chemical name: Di-μ-chloro-bis{chloro[hydrotris(pyrazol-1- yl)borato)](tetrahydrofuran)ytterbium(III)] toluene solvate
• Formula: C33 H44 B2 Cl4 N12 O2 Yb2
• Calculated formula: C33 H36 B2 Cl4 N12 O2 Yb2
• Title of publication: Di-μ-chloro-bis{chloro[hydrotris(pyrazol-1-yl)borato)](tetrahydrofuran)ytterbium(III)} toluene solvate
• Authors of publication: Rabe, Gerd W.; Zhang-Presse, Mei; Riederer, Florian A.; Rheingold, Arnold L.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 11
• Pages of publication: m3149 - m3151
• a: 9.209 ± 0.003 Å
• b: 10.919 ± 0.003 Å
• c: 11.881 ± 0.003 Å
• α: 105.733 ± 0.004°
• β: 105.648 ± 0.004°
• γ: 103.25 ± 0.004°
• Cell volume: 1046.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0408
• Weighted residual factors for significantly intense reflections: 0.1031
• Weighted residual factors for all reflections included in the refinement: 0.1041
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes