Information card for entry 2212764

Structure parameters

• Chemical name: Bis{N-[bis(6-bromopyridin-2-yl)methylene-κN]ethane-1,2-diamine- κ^2^N,N'}nickel(II) bis(perchlorate)
• Formula: C26 H24 Br4 Cl2 N8 Ni O8
• Calculated formula: C26 H24 Br4 Cl2 N8 Ni O8
• SMILES: C1(c2cccc(n2)Br)c2cccc([n]2[Ni]234([N]=1CC[NH2]2)[n]1c(C(c2cccc(n2)Br)=[N]3CC[NH2]4)cccc1Br)Br.[O-]Cl(=O)(=O)=O.[O-]Cl(=O)(=O)=O
• Title of publication: Bis{<i>N</i>-[bis(6-bromopyridin-2-yl)methylene-κ<i>N</i>]ethane-1,2-diamine-κ^2^<i>N</i>,<i>N</i>'}nickel(II) bis(perchlorate)
• Authors of publication: Knight, James C.; Amoroso, Angelo J.; Prabaharan, Ravi; Edwards, Peter G.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 4
• Pages of publication: m1046 - m1047
• a: 9.1897 ± 0.0003 Å
• b: 12.9937 ± 0.0003 Å
• c: 15.0869 ± 0.0005 Å
• α: 110.077 ± 0.002°
• β: 95.308 ± 0.002°
• γ: 94.573 ± 0.002°
• Cell volume: 1672.76 ± 0.09 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1171
• Residual factor for significantly intense reflections: 0.0638
• Weighted residual factors for significantly intense reflections: 0.1288
• Weighted residual factors for all reflections included in the refinement: 0.1483
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes