Information card for entry 2214330

Structure parameters

• Chemical name: μ~3~-Iodido-tri-μ~3~-sulfido- tris[(triphenylphosphine)silver(I)][thioxotungsten(VI)] dichloromethane 0.45-solvate
• Formula: C54.45 H45.9 Ag3 Cl0.9 I P3 S4 W
• Calculated formula: C54.449 H45.898 Ag3 Cl0.898 I P3 S4 W
• Title of publication: μ~3~-Iodido-tri-μ~3~-sulfido-tris[(triphenylphosphine)silver(I)][thioxotungsten(VI)] dichloromethane 0.45-solvate
• Authors of publication: Beheshti, Azizolla; Clegg, William; Dale, Sophie H.; Hyvadi, Reza
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 7
• Pages of publication: m1990 - m1991
• a: 12.113 ± 0.003 Å
• b: 13.3231 ± 0.0014 Å
• c: 20.0301 ± 0.0014 Å
• α: 74.671 ± 0.008°
• β: 87.659 ± 0.011°
• γ: 63.692 ± 0.01°
• Cell volume: 2783.7 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0426
• Residual factor for significantly intense reflections: 0.028
• Weighted residual factors for significantly intense reflections: 0.062
• Weighted residual factors for all reflections included in the refinement: 0.0679
• Goodness-of-fit parameter for all reflections included in the refinement: 0.984
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes