Information card for entry 2214369

Structure parameters

• Chemical name: Bis[N-ethyl-N'-(pyridin-2-ylmethylene)ethane-1,2-diamine]nickel(II) bis(perchlorate)
• Formula: C20 H30 Cl2 N6 Ni O8
• Calculated formula: C20 H30 Cl2 N6 Ni O8
• Title of publication: Bis[<i>N</i>-ethyl-<i>N</i>'-(pyridin-2-ylmethylene)ethane-1,2-diamine]nickel(II) bis(perchlorate)
• Authors of publication: Zhe Hong
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 7
• Pages of publication: m2026 - m2026
• a: 21.1172 ± 0.0018 Å
• b: 16.8787 ± 0.0014 Å
• c: 12.0819 ± 0.001 Å
• α: 90°
• β: 105.531 ± 0.001°
• γ: 90°
• Cell volume: 4149.1 ± 0.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.097
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1609
• Weighted residual factors for all reflections included in the refinement: 0.1894
• Goodness-of-fit parameter for all reflections included in the refinement: 0.989
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes