Information card for entry 2214385

Structure parameters

• Chemical name: Bis(dimethylformamide-2κO)bis[μ-1-(2-oxidobenzoyl)-2- (phenoxyacetyl)hydrazine(3-)]- 1κ^3^O,N,O':2κ^2^N,O'';2κ^2^N,O'':3κ^3^O,N,O'-dipyridine-1κN,3κN- trinickel(II)
• Formula: C46 H46 N8 Ni3 O10
• Calculated formula: C46 H46 N8 Ni3 O10
• SMILES: c12c(cccc1)C1=[N]3[N](=C(COc4ccccc4)O[Ni]3([n]3ccccc3)O2)[Ni]2(O1)([O]=CN(C)C)([N]1=C(COc3ccccc3)O[Ni]3([N]1=C(c1c(cccc1)O3)O2)[n]1ccccc1)[O]=CN(C)C
• Title of publication: Bis(dimethylformamide-2κ<i>O</i>)bis[μ-1-(2-oxidobenzoyl)-2-(phenoxyacetyl)hydrazine(3{-})]-1κ^3^<i>O</i>,<i>N</i>,<i>O</i>':2κ^2^<i>N</i>,<i>O</i>'';2κ^2^<i>N</i>,<i>O</i>'':3κ^3^<i>O</i>,<i>N</i>,<i>O</i>'-dipyridine-1κ<i>N</i>,3κ<i>N</i>-trinickel(II)
• Authors of publication: Zhao, Yan; Luo, Jian-Hai; Huang, Xi-He; Huang, Chang-Cang; Liu, Dong-Sheng
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 7
• Pages of publication: m1999 - m2000
• a: 28.646 ± 0.006 Å
• b: 8.249 ± 0.0016 Å
• c: 21.176 ± 0.004 Å
• α: 90°
• β: 112.98 ± 0.03°
• γ: 90°
• Cell volume: 4606.8 ± 1.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1091
• Residual factor for significantly intense reflections: 0.06
• Weighted residual factors for significantly intense reflections: 0.1098
• Weighted residual factors for all reflections included in the refinement: 0.1291
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes