Information card for entry 2214391

Structure parameters

• Chemical name: Bis(μ-4-benzyl-3,5-diphenylpyrazolato-κ^2^<i>N</i>:<i>N</i>')bis[(4,4'-\ dimethyl-2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')palladium(II)] bis(hexafluoridophosphate) diethyl ether monosolvate monohydrate
• Formula: C72 H70 F12 N8 O2 P2 Pd2
• Calculated formula: C72 H70 F12 N8 O2 P2 Pd2
• Title of publication: Bis(μ-4-benzyl-3,5-diphenylpyrazolato-κ^2^<i>N</i>:<i>N</i>')bis[(4,4'-dimethyl-2,2'-bipyridine-κ^2^<i>N</i>,<i>N</i>')palladium(II)] bis(hexafluorophosphate) diethyl ether monosolvate monohydrate
• Authors of publication: Hai-Ping Huang; Li-Xia Liu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 7
• Pages of publication: m1875 - m1876
• a: 22.1138 ± 0.0003 Å
• b: 22.1138 ± 0.0003 Å
• c: 12.8884 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5458.29 ± 0.13 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291 ± 2 K
• Number of distinct elements: 7
• Space group number: 152
• Hermann-Mauguin space group symbol: P 31 2 1
• Hall space group symbol: P 31 2"
• Residual factor for all reflections: 0.053
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.1321
• Weighted residual factors for all reflections included in the refinement: 0.1435
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes