Information card for entry 2214747

Structure parameters

• Chemical name: [μ-1,2-Disalicyloylhydrazine(2-)- κ^3^N,O,O':κ^3^N',O'',O''']bis[tripyridinenickel(II)] pyridine disolvate
• Formula: C54 H48 N10 Ni2 O4
• Calculated formula: C54 H48 N10 Ni2 O4
• SMILES: c12ccccc2C2=[N]3[Ni]([n]4ccccc4)([n]4ccccc4)([n]4ccccc4)(O1)OC1c4c(cccc4)O[Ni]([N]3=1)([n]1ccccc1)([n]1ccccc1)([n]1ccccc1)O2.n1ccccc1.n1ccccc1
• Title of publication: [μ-1,2-Disalicyloylhydrazine(2–)-κ^3^<i>N</i>,<i>O</i>,<i>O</i>':κ^3^<i>N</i>',<i>O</i>'',<i>O</i>''']bis[tripyridinenickel(II)] pyridine disolvate
• Authors of publication: Yuting Chen; Jian-Min Dou; Da-Cheng Li; Da-Qi Wang; Yue-Hua Zhu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 8
• Pages of publication: m2118 - m2118
• a: 27.04 ± 0.002 Å
• b: 27.04 ± 0.002 Å
• c: 14.3178 ± 0.0018 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10468.6 ± 1.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0916
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1328
• Weighted residual factors for all reflections included in the refinement: 0.1516
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes