Information card for entry 2214824

Structure parameters

• Chemical name: Di-μ-azido-κ^4^N:N-bis[(azido-κN)(2,9-dimethyl-1,10-phenanthroline- κN,N)nickel(II)]
• Formula: C28 H24 N16 Ni2
• Calculated formula: C28 H24 N16 Ni2
• SMILES: c1(ccc2ccc3ccc([n]4c3c2[n]1[Ni]14([N](=N#N)[Ni]2([n]3c(C)ccc4ccc5ccc([n]2c5c34)C)([N]1=N#N)N=N#N)N=N#N)C)C
• Title of publication: Di-μ-azido-κ^4^<i>N</i>:<i>N</i>-bis[(azido-κ<i>N</i>)(2,9-dimethyl-1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')nickel(II)]
• Authors of publication: Li, Ling-Ling; Liu, Tian-Fu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 8
• Pages of publication: m2211 - m2211
• a: 13.471 ± 0.003 Å
• b: 11.226 ± 0.002 Å
• c: 19.605 ± 0.004 Å
• α: 90°
• β: 94.36 ± 0.03°
• γ: 90°
• Cell volume: 2956.2 ± 1 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0804
• Residual factor for significantly intense reflections: 0.0332
• Weighted residual factors for significantly intense reflections: 0.0726
• Weighted residual factors for all reflections included in the refinement: 0.0825
• Goodness-of-fit parameter for all reflections included in the refinement: 0.93
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes