Information card for entry 2215776

Structure parameters

• Chemical name: <i>cyclo</i>-Tetrakis[μ-<i>N</i>-(2-hydroxybenzoyl)-<i>N</i>'-(2-hydroxy-3-\ methoxybenzylidene)hydrazinato(2-)]tetranickel(II) <i>N</i>,<i>N</i>-dimethylformamide tetrasolvate
• Formula: C72 H76 N12 Ni4 O20
• Calculated formula: C72 H76 N12 Ni4 O20
• SMILES: CN(C)C=O.C[O]1c2cccc3c2[O]2[Ni]456(OC(=N[N]4=C3)c3ccccc3O)[Ni]3478OC(=N[N]3=Cc3cccc9[O](C)[Ni]%10%11(OC(=N[N]%10=Cc%10cccc([O]5C)c%10[O]6%11)c5ccccc5O)([O]4c39)[Ni]3412OC(=N[N]3=Cc1cccc([O]7C)c1[O]84)c1ccccc1O)c1ccccc1O.CN(C)C=O.CN(C)C=O.CN(C)C=O
• Title of publication: <i>cyclo</i>-Tetrakis[μ-<i>N</i>-(2-hydroxybenzoyl)-<i>N</i>'-(2-hydroxy-3-methoxybenzylidene)hydrazinato(2{-})]tetranickel(II) <i>N</i>,<i>N</i>-dimethylformamide tetrasolvate
• Authors of publication: Guan, Guizhi; Gao, Yuxiang; Wang, Lixia; Wang, Tao
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 11
• Pages of publication: m2662 - m2662
• a: 24.1627 ± 0.0005 Å
• b: 24.1627 ± 0.001 Å
• c: 13.0428 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7614.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0899
• Residual factor for significantly intense reflections: 0.0415
• Weighted residual factors for significantly intense reflections: 0.1084
• Weighted residual factors for all reflections included in the refinement: 0.1479
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes