Information card for entry 2216199

Structure parameters

• Chemical name: Triacetonitrile(1,1,4,7,7-pentamethyldiethylenetriamine)nickel(II) bis(hexafluoridophosphate)
• Formula: C15 H32 F12 N6 Ni P2
• Calculated formula: C15 H32 F12 N6 Ni P2
• Title of publication: Triacetonitrile(1,1,4,7,7-pentamethyldiethylenetriamine)nickel(II) bis(hexafluoridophosphate)
• Authors of publication: Morawitz, Thorsten; Lerner, Hans-Wolfram; Bolte, Michael
• Journal of publication: Acta Crystallographica, Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 12
• Pages of publication: o4551 - o4551
• a: 17.4418 ± 0.0008 Å
• b: 10.5913 ± 0.0006 Å
• c: 15.7326 ± 0.0008 Å
• α: 90°
• β: 110.921 ± 0.004°
• γ: 90°
• Cell volume: 2714.7 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0483
• Weighted residual factors for significantly intense reflections: 0.1241
• Weighted residual factors for all reflections included in the refinement: 0.1303
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No