Information card for entry 2216612

Structure parameters

• Chemical name: [μ-1,2-Bis(2-hydroxybenzoyl)hydrazine(4-)]bis[tripyridinecobalt(II)] bis[trichloridopyridinecobalt(III)]
• Formula: C54 H48 Cl6 Co4 N10 O4
• Calculated formula: C54 H48 Cl6 Co4 N10 O4
• SMILES: c1[n](cccc1)[Co]12([n]3ccccc3)(OC3c4c(cccc4)O[Co]4([N]=3[N]1=C(c1c(cccc1)O2)O4)([n]1ccccc1)([n]1ccccc1)[n]1ccccc1)[n]1ccccc1.[n]1(ccccc1)[Co](Cl)(Cl)Cl.[n]1(ccccc1)[Co](Cl)(Cl)Cl
• Title of publication: [μ-1,2-Bis(2-hydroxybenzoyl)hydrazine(4‒)]bis[tripyridinecobalt(II)] bis[trichloridopyridinecobalt(III)]
• Authors of publication: Yu-Ting Chen; Jian-Min Dou; Da-Cheng Li; Da-Qi Wang; Yue-Hua Zhu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 12
• Pages of publication: m3129 - m3130
• a: 16.5112 ± 0.0018 Å
• b: 10.7135 ± 0.0015 Å
• c: 17.975 ± 0.002 Å
• α: 90°
• β: 66.078 ± 0.002°
• γ: 90°
• Cell volume: 2906.5 ± 0.6 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1497
• Residual factor for significantly intense reflections: 0.0635
• Weighted residual factors for significantly intense reflections: 0.131
• Weighted residual factors for all reflections included in the refinement: 0.1608
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes