Information card for entry 2216777

Structure parameters

• Chemical name: N'-(3,3,7,7-Tetramethyl-1,5-dioxaspiro[5,5]undecane-8-ylidene)- p-toluenesulfonohydrazide
• Formula: C20 H30 N2 O4 S
• Calculated formula: C20 H30 N2 O4 S
• SMILES: S(=O)(=O)(N/N=C1CCCC2(OCC(CO2)(C)C)C\1(C)C)c1ccc(cc1)C
• Title of publication: <i>N</i>'-(3,3,7,7-Tetramethyl-1,5-dioxaspiro[5,5]undecane-8-ylidene)-<i>p</i>-toluenesulfonohydrazide
• Authors of publication: Zhu, Xiaolei; Zou, Liwei; Xu, Yongting; Han, Jing; Zhang, Chenglu
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 12
• Pages of publication: o4931 - o4931
• a: 7.437 ± 0.002 Å
• b: 10.045 ± 0.003 Å
• c: 14.299 ± 0.004 Å
• α: 98.397 ± 0.004°
• β: 92.789 ± 0.004°
• γ: 98.676 ± 0.003°
• Cell volume: 1041.9 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.1191
• Weighted residual factors for all reflections included in the refinement: 0.1268
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes