Information card for entry 2217714

Structure parameters

• Chemical name: [N,N'-(1,2-Diphenylethane-1,2-diyl)bis(pyridine-2-carboxamidato)]nickel(II) diethyl ether hemisolvate
• Formula: C28 H25 N4 Ni O2.5
• Calculated formula: C28 H25 N4 Ni O2.5
• Title of publication: [<i>N</i>,<i>N</i>'-(1,2-Diphenylethane-1,2-diyl)bis(pyridine-2-carboxamidato)]nickel(II) diethyl ether hemisolvate
• Authors of publication: Yang, Li; Deng, Dong-Yan; Li, Mei; Zhou, Xiang-Ge
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 3
• Pages of publication: m439
• a: 21.838 ± 0.003 Å
• b: 11.1675 ± 0.0015 Å
• c: 11.0443 ± 0.0015 Å
• α: 90°
• β: 100.949 ± 0.003°
• γ: 90°
• Cell volume: 2644.4 ± 0.6 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.1274
• Residual factor for significantly intense reflections: 0.0583
• Weighted residual factors for significantly intense reflections: 0.1325
• Weighted residual factors for all reflections included in the refinement: 0.1621
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes