Information card for entry 2218429

Structure parameters

• Chemical name: {μ-6,6'-diethoxy-2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato- 1κ^4^O^1^,<i>O</i>^1'^,<i>O</i>^6^,<i>O</i>^6'^: 2κ^4^O^1^,<i>N</i>,<i>N</i>',O^1'^'}trinitrato-1κ^6^O,<i>O</i>'-holmium(III) nickel(II))
• Formula: C20 H22 Ho N5 Ni O13
• Title of publication: {μ-6,6'-Diethoxy-2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}trinitratoholmium(III)nickel(II)
• Authors of publication: Xiao, Yi-An; Fu, Xiang-Kai; Sui, Yan; Wu, Qing; Xiong, Shao-Hui
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 6
• Pages of publication: m806 - m807
• a: 8.5825 ± 0.0008 Å
• b: 13.7028 ± 0.0014 Å
• c: 21.203 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2493.6 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0647
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1033
• Weighted residual factors for all reflections included in the refinement: 0.1131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: No
• Has disorder: No
• Has Fobs: Yes