Information card for entry 2220679
| Chemical name |
bis{μ-3,3'-(1,3,4-thiadiazole-2,5- diyldithio)bis[pentanedionato(1-)]}bis[diaquanickel(II)] dimethylformamide disolvate trihydrate |
| Formula |
C30 H52 N6 Ni2 O17 S6 |
| Calculated formula |
C30 H52 N6 Ni2 O17 S6 |
| Title of publication |
Bis{μ-3,3'-(1,3,4-thiadiazole-2,5-diyldithio)bis[pentanedionato(1{-})]}bis[diaquanickel(II)] dimethylformamide disolvate trihydrate |
| Authors of publication |
Jian, Fang-Fang; Han, Song-Jiang |
| Journal of publication |
Acta Crystallographica Section E |
| Year of publication |
2009 |
| Journal volume |
65 |
| Journal issue |
2 |
| Pages of publication |
m207 |
| a |
10.582 ± 0.002 Å |
| b |
11.469 ± 0.001 Å |
| c |
12.136 ± 0.002 Å |
| α |
102.3 ± 0.03° |
| β |
107.21 ± 0.01° |
| γ |
116.26 ± 0.03° |
| Cell volume |
1155.6 ± 0.6 Å3 |
| Cell temperature |
295 ± 2 K |
| Ambient diffraction temperature |
295 ± 2 K |
| Number of distinct elements |
6 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0417 |
| Residual factor for significantly intense reflections |
0.0349 |
| Weighted residual factors for significantly intense reflections |
0.0897 |
| Weighted residual factors for all reflections included in the refinement |
0.0946 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.034 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
Yes |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/2220679.html
