Information card for entry 2221371

Structure parameters

• Chemical name: {μ-6,6'-Dimethoxy-2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato- 1κ^4^<i>O</i>^6^,<i>O</i>^1^,<i>O</i>^1'^,<i>O</i>^6'^: 2κ^4^<i>O</i>^1^,<i>N</i>,<i>N</i>',<i>O</i>^1'^}(methanol- 1κ<i>O</i>)(perchlorato-1κ<i>O</i>)nickel(II)sodium
• Formula: C19 H22 Cl N2 Na Ni O9
• Calculated formula: C19 H22 Cl N2 Na Ni O9
• SMILES: [N]12=Cc3c(c(ccc3)[O]([Na]345(OCl(=O)(=O)=O)[OH]C)C)[O]3[Ni]32[N](=Cc2cccc(c2[O]34)[O]5C)CC1
• Title of publication: {μ-6,6'-Dimethoxy-2,2'-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato-1κ^4^<i>O</i>^6^,<i>O</i>^1^,<i>O</i>^1'^,<i>O</i>^6'^:2κ^4^<i>O</i>^1^,<i>N</i>,<i>N</i>',<i>O</i>^1'^}(methanol-1κ<i>O</i>)(perchlorato-1κ<i>O</i>)nickel(II)sodium
• Authors of publication: Xiao, Hui-Quan
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 4
• Pages of publication: m400
• a: 12.026 ± 0.002 Å
• b: 8.136 ± 0.0016 Å
• c: 23.394 ± 0.005 Å
• α: 90°
• β: 104.302 ± 0.003°
• γ: 90°
• Cell volume: 2218 ± 0.7 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0527
• Weighted residual factors for significantly intense reflections: 0.147
• Weighted residual factors for all reflections included in the refinement: 0.1591
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes