Information card for entry 2221909

Structure parameters

• Chemical name: [13,27-Dichloro-3,6,9,17,20,23- hexaazatetracyclo[23.3.1.1^11,15^.0^2,6^]triaconta- 1(29),9,11,13,15(30),16,23,25,27-nonaene-29,30-diol- κ^5^<i>N</i>^17^,<i>N</i>^20^,<i>N</i>^23^,<i>O</i>^29^,<i>O</i>^30^] bis(nitrato-κ^2^<i>O</i>,<i>O</i>')europium(III) nitrate methanol hemisolvate
• Formula: C24.5 H30 Cl2 Eu N9 O11.5
• Calculated formula: C24.5 H30 Cl2 Eu N9 O11.5
• Title of publication: [13,27-Dichloro-3,6,9,17,20,23-hexaazatetracyclo[23.3.1.1^11,15^.0^2,6^]triaconta-1(29),9,11,13,15(30),16,23,25,27-nonaene-29,30-diol-κ^5^<i>N</i>^17^,<i>N</i>^20^,<i>N</i>^23^,<i>O</i>^29^,<i>O</i>^30^]bis(nitrato-κ^2^<i>O</i>,<i>O</i>')europium(III) nitrate methanol hemisolvate
• Authors of publication: Yue, Xia-Li
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 6
• Pages of publication: m614
• a: 23.7371 ± 0.0016 Å
• b: 14.3327 ± 0.001 Å
• c: 19.388 ± 0.0013 Å
• α: 90°
• β: 91.804 ± 0.001°
• γ: 90°
• Cell volume: 6592.9 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0399
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for significantly intense reflections: 0.0831
• Weighted residual factors for all reflections included in the refinement: 0.0884
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes