Information card for entry 2222752

Structure parameters

• Chemical name: (μ-Pyridine-2-carbaldehyde azine)bis[bis(triphenylphosphine-κ<i>P</i>)copper(I)] bis(tetrafluoroborate) dichloromethane disolvate
• Formula: C86 H74 B2 Cl4 Cu2 F8 N4 P4
• Calculated formula: C86 H74 B2 Cl4 Cu2 F8 N4 P4
• Title of publication: (μ-Pyridine-2-carbaldehyde azine)bis[bis(triphenylphosphine-κ<i>P</i>)copper(I)] bis(tetrafluoridoborate) dichloromethane disolvate
• Authors of publication: Yang, Li; Xie, Yu; Zou, Jianping; Jia, Jie; Hong, Xiaowei
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 8
• Pages of publication: m1017
• a: 13.0932 ± 0.0016 Å
• b: 27.501 ± 0.003 Å
• c: 13.9033 ± 0.0018 Å
• α: 90°
• β: 115.117 ± 0.002°
• γ: 90°
• Cell volume: 4532.9 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1418
• Residual factor for significantly intense reflections: 0.0809
• Weighted residual factors for significantly intense reflections: 0.2319
• Weighted residual factors for all reflections included in the refinement: 0.2676
• Goodness-of-fit parameter for all reflections included in the refinement: 0.954
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes