Information card for entry 2223378

Structure parameters

• Chemical name: Tetrakis(6-methyl-2,2'-bipyridine)-1κ^2^<i>N</i>,<i>N</i>'; 2κ^2^<i>N</i>,<i>N</i>';3κ^2^<i>N</i>,<i>N</i>';4κ^2^<i>N</i>,<i>N</i>'- tetra-μ-nitrato-1:2κ^2^<i>O</i>:<i>O</i>';2:3κ^3^<i>O</i>: <i>O</i>',<i>O</i>'';2:3κ^3^<i>O</i>,<i>O</i>':<i>O</i>''; 3:4κ^2^<i>O</i>:<i>O</i>'-tetranitrato- 1κ^4^<i>O</i>,<i>O</i>';4κ^2^<i>O</i>,<i>O</i>'-tetralead(II)
• Formula: C22 H20 N8 O12 Pb2
• Calculated formula: C22 H20 N8 O12 Pb2
• SMILES: Cc1cccc2c3cccc[n]3[Pb]3([n]12)(ON(=O)=[O]3)ON(=O)=[O][Pb]12([n]3c(C)cccc3c3[n]1cccc3)(ON(=O)=O)ON(=O)=[O]2
• Title of publication: Tetrakis(6-methyl-2,2'-bipyridine)-1κ^2^<i>N</i>,<i>N</i>';2κ^2^<i>N</i>,<i>N</i>';3κ^2^<i>N</i>,<i>N</i>';4κ^2^<i>N</i>,<i>N</i>'-tetra-μ-nitrato-1:2κ^2^<i>O</i>:<i>O</i>';2:3κ^3^<i>O</i>:<i>O</i>',<i>O</i>'';2:3κ^3^<i>O</i>,<i>O</i>':<i>O</i>'';3:4κ^2^<i>O</i>:<i>O</i>'-tetranitrato-1κ^4^<i>O</i>,<i>O</i>';4κ^2^<i>O</i>,<i>O</i>'-tetralead(II)
• Authors of publication: Ahmadi, Roya; Kalateh, Khadijeh; Alizadeh, Robabeh; Khoshtarkib, Zeinab; Amani, Vahid
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 10
• Pages of publication: m1169 - m1170
• a: 11.093 ± 0.002 Å
• b: 11.266 ± 0.002 Å
• c: 12.642 ± 0.003 Å
• α: 109.25 ± 0.03°
• β: 95.43 ± 0.03°
• γ: 105.62 ± 0.03°
• Cell volume: 1407 ± 0.7 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0607
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.1292
• Weighted residual factors for all reflections included in the refinement: 0.1368
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes