Information card for entry 2224123

Structure parameters

• Chemical name: <i>catena</i>-Poly[[[bis(<i>N</i>,<i>N</i>-dimethylformamide)iron(II)]- {μ-2,2'-bis(diphenylphosphinoyl)-<i>N</i>,<i>N</i>'-[(1<i>R</i>,2<i>R</i>)- cyclohexane-1,2-diyl]dibenzamide}] bis(perchlorate) <i>N</i>,<i>N</i>-dimethylformamide disolvate]
• Formula: C56 H68 Cl2 Fe N6 O16 P2
• Calculated formula: C56 H68 Cl2 Fe N6 O16 P2
• Title of publication: <i>catena</i>-Poly[[[bis(<i>N</i>,<i>N</i>-dimethylformamide)iron(II)]-{μ-2,2'-bis(diphenylphosphinoyl)-<i>N</i>,<i>N</i>'-[(1<i>R</i>,2<i>R</i>)-cyclohexane-1,2-diyl]dibenzamide}] bis(perchlorate) <i>N</i>,<i>N</i>-dimethylformamide disolvate]
• Authors of publication: Ferrell, Grant R.; Moore, Curtis; Rheingold, Arnold L.; Daley, Christopher J. A.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 12
• Pages of publication: m1512 - m1513
• a: 10.9725 ± 0.0004 Å
• b: 15.4417 ± 0.0006 Å
• c: 36.2173 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6136.4 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0928
• Residual factor for significantly intense reflections: 0.0691
• Weighted residual factors for significantly intense reflections: 0.1794
• Weighted residual factors for all reflections included in the refinement: 0.1968
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes