Information card for entry 2224478

Structure parameters

• Chemical name: Di-μ-iodido-bis[acetyl(4-methyl-2,6,7-trioxa-1- phosphabicyclo[2.2.2]octane)(<i>N</i>-nitroso-<i>N</i>-oxidoaniline- κ^2^<i>O</i>,<i>O</i>')rhodium(III)]
• Formula: C26 H34 I2 N4 O12 P2 Rh2
• Calculated formula: C26 H34 I2 N4 O12 P2 Rh2
• SMILES: [P]12(OCC(CO2)(CO1)C)[Rh]12(C(=O)C)([O]=NN(O2)c2ccccc2)[I][Rh]2([I]1)([P]13OCC(CO3)(CO1)C)(C(=O)C)ON(N=[O]2)c1ccccc1
• Title of publication: Di-μ-iodido-bis[acetyl(4-methyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane)(<i>N</i>-nitroso-<i>N</i>-oxidoaniline-κ^2^<i>O</i>,<i>O</i>')rhodium(III)]
• Authors of publication: Venter, Johan A.; Purcell, W.; Visser, H. G.
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 12
• Pages of publication: m1528 - m1529
• a: 10.055 ± 0.002 Å
• b: 16.944 ± 0.003 Å
• c: 11.149 ± 0.002 Å
• α: 90°
• β: 112.75 ± 0.03°
• γ: 90°
• Cell volume: 1751.7 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0327
• Weighted residual factors for all reflections included in the refinement: 0.0754
• Goodness-of-fit parameter for all reflections included in the refinement: 0.951
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes