Information card for entry 2225428

Structure parameters

• Chemical name: (Triphenylphosphine-κ<i>P</i>)[1,1,1-tris(diphenylphosphinomethyl)ethane- κ^3^<i>P</i>,<i>P</i>',<i>P</i>'']copper(I) tetrafluoridoborate
• Formula: C59 H54 B Cu F4 P4
• Calculated formula: C59 H54 B Cu F4 P4
• Title of publication: (Triphenylphosphine-κ<i>P</i>)[1,1,1-tris(diphenylphosphinomethyl)ethane-κ^3^<i>P</i>,<i>P</i>',<i>P</i>'']copper(I) tetrafluoridoborate
• Authors of publication: Yin, Qi; Gan, Xin
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 4
• Pages of publication: m369
• a: 13.47 ± 0.004 Å
• b: 14.356 ± 0.004 Å
• c: 26.24 ± 0.007 Å
• α: 90°
• β: 91.338 ± 0.005°
• γ: 90°
• Cell volume: 5073 ± 2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1276
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1127
• Weighted residual factors for all reflections included in the refinement: 0.1383
• Goodness-of-fit parameter for all reflections included in the refinement: 0.977
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes