Information card for entry 2226177

Structure parameters

• Chemical name: (+)-{1,2-Bis[(2<i>R</i>,5<i>R</i>)-2,5-dimethylphospholan-1-yl]ethane- κ^2^<i>P</i>,<i>P</i>'}(η^4^-cycloocta-1,5-diene)rhodium(I) tetrafluoridoborate
• Formula: C22 H40 B F4 P2 Rh
• Calculated formula: C22 H40 B F4 P2 Rh
• Title of publication: (+)-{1,2-Bis[(2<i>R</i>,5<i>R</i>)-2,5-dimethylphospholan-1-yl]ethane-κ^2^<i>P</i>,<i>P</i>'}(η^4^-cycloocta-1,5-diene)rhodium(I) tetrafluoridoborate
• Authors of publication: Schulz, Stefan; Drexler, Hans-Joachim; Heller, Detlef
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 6
• Pages of publication: m721 - m722
• a: 10.224 ± 0.002 Å
• b: 14.771 ± 0.003 Å
• c: 50.158 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7575 ± 3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0493
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0445
• Weighted residual factors for all reflections included in the refinement: 0.046
• Goodness-of-fit parameter for all reflections included in the refinement: 0.872
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes