Information card for entry 2226735

Structure parameters

• Chemical name: <i>catena</i>-Poly[[(1,10-phenanthroline-κ<i>N</i>,<i>N</i>')lead(II)]-μ- azido-κ^2^<i>N</i>^1^:<i>N</i>^3^-μ-nitrito- κ^3^<i>O</i>,<i>O</i>':<i>O</i>'-[(1,10-phenanthroline- κ<i>N</i>,<i>N</i>')lead(II)]-di-μ-azido-κ^4^<i>N</i>^1^:<i>N</i>^1^]
• Formula: C24 H16 N14 O2 Pb2
• Calculated formula: C24 H16 N14 O2 Pb2
• Title of publication: <i>catena</i>-Poly[[(1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')lead(II)]-μ-azido-κ^2^<i>N</i>^1^:<i>N</i>^3^-μ-nitrito-κ^3^<i>O</i>,<i>O</i>':<i>O</i>'-[(1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')lead(II)]-di-μ-azido-κ^4^<i>N</i>^1^:<i>N</i>^1^]
• Authors of publication: Mohammadnezhad, Gholamhossein; Ghanbarpour, Ali Reza; Amini, Mostafa M.; Ng, Seik Weng
• Journal of publication: Acta Crystallographica Section E
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 7
• Pages of publication: m821
• a: 7.686 ± 0.0005 Å
• b: 9.2056 ± 0.0006 Å
• c: 9.908 ± 0.0007 Å
• α: 90.541 ± 0.001°
• β: 109.665 ± 0.001°
• γ: 104.626 ± 0.001°
• Cell volume: 635.32 ± 0.07 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0303
• Residual factor for significantly intense reflections: 0.0276
• Weighted residual factors for significantly intense reflections: 0.0694
• Weighted residual factors for all reflections included in the refinement: 0.0706
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes